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ZELWYCSDHIFMOP-HAPIZUAHSA-N synthesis

11synthesis methods

Product Name:ZELWYCSDHIFMOP-HAPIZUAHSA-N
CAS Number:59699-82-0
Molecular formula:C22H32O2
Molecular Weight:328.4883

40834-42-2 Synthesis

40834-42-2
179 suppliers
$27.00/1g

59699-82-0
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Yield:-

Steps:

Multi-step reaction with 9 steps
1: 1.) NaH / 1.) HMPA, 0 deg C, 1 h, 2.) 20 min
2: 1.) ethylmagnesium bromide / 1.) THF, room temperature, 1 h, 2.) 15 min
3: 75 percent / DIBAH / tetrahydrofuran; toluene / 0.5 h / -78 °C
4: 90 percent / H₂ / Lindlar catalyst / methanol / 24 h
5: 80 percent / imidazole / dimethylformamide / 18 h / Ambient temperature
6: 90 percent / LiAlH₄, TiCl₃ / tetrahydrofuran / 0.5 h / Ambient temperature
7: sodium fluoride, pyridinium fluoride / tetrahydrofuran; acetonitrile / 5 h / Ambient temperature
8: MnO₂ / CCl₄ / 0.5 h
9: 60 percent / NaCN, AgO, MnO₂ / 14 h / 40 °C

References:

Solladie, Guy;Girardin, Andre;Lang, Gerard [Journal of Organic Chemistry,1989,vol. 54,# 11,p. 2620 - 2628]

25576-25-4 Synthesis

1,3,3-TriMethyl-2-[(1E,3E)-3-Methyl-1,3-hexadien-5-ynyl]-cyclohexane

25576-25-4
11 suppliers
$1230.00/100mg

2-Butenoic acid, 3-[[(trifluoromethyl)sulfonyl]oxy]-, ethyl ester, (2Z)-

122135-84-6
0 suppliers
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59699-82-0
6 suppliers
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References

64-17-5 Synthesis

64-17-5
891 suppliers
$10.00/50g

472-86-6
44 suppliers
$375.00/10mg

59699-82-0
6 suppliers
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References

1-Penten-4-yn-3-ol, 3-methyl-1-(2,6,6-trimethyl-1-cyclohexen-1-yl)-, (1E)-

17974-59-3
0 suppliers
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59699-82-0
6 suppliers
inquiry

References

2-Butenoic acid, 3-Methyl-4-oxo-, Methyl ester, (Z)-

96928-85-7
9 suppliers
inquiry

59699-82-0
6 suppliers
inquiry

References

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ZELWYCSDHIFMOP-HAPIZUAHSA-N synthesis