2-Methyl-2-nitropropan-1-ol
|
|
|
- CAS-Nr.
- 76-39-1
- Bezeichnung:
- 2-Methyl-2-nitropropan-1-ol
- Englisch Name:
- 2-Methyl-2-nitropropan-1-ol
- Synonyma:
- 1-Propanol, 2-methyl-2-nitro-;2-Methyl-2-nitropropanol;2-methyl-2-nitro-1-propano;2-METHYL-2-NITRO-1-PROPANOL;2-NITRO-2-METHYL-1-PROPANOL;2-NITROISOBUTANOL;Methylnitropropanol;methyl-2nitro-2propanol;2-Nitro-2-methylpropanol;2-methyl-2-nitropropan-1-ol
- CBNumber:
- CB3474945
- Summenformel:
- C4H9NO3
- Molgewicht:
- 119.12
- MOL-Datei:
- 76-39-1.mol
|
2-Methyl-2-nitropropan-1-ol Eigenschaften
- Schmelzpunkt:
- 86-89 °C(lit.)
- Siedepunkt:
- 94-95 °C10 mm Hg(lit.)
- Dichte
- 1.0765 (estimate)
- Brechungsindex
- 1.4413 (estimate)
- pka
- 13.79±0.10(Predicted)
- InChI
- InChI=1S/C4H9NO3/c1-4(2,3-6)5(7)8/h6H,3H2,1-2H3
- InChIKey
- MVGJRISPEUZYAQ-UHFFFAOYSA-N
- SMILES
- C(O)C(C)([N+]([O-])=O)C
- NIST chemische Informationen
- 1-Propanol, 2-methyl-2-nitro-(76-39-1)
- EPA chemische Informationen
- 1-Propanol, 2-methyl-2-nitro- (76-39-1)
2-Methyl-2-nitropropan-1-ol Chemische Eigenschaften,Einsatz,Produktion Methoden
Synthese
By catalyst 10g (Ti-V-ZSM-5), acetone 58.08g, ammonium hydroxide 20g are
added in 400ml methanol, are warming up to 70
DEG C, hydrogen peroxide (35%) 226.7g is slowly added dropwise,
temperature is maintained to react 1h at 65-75°C, obtain 2- nitros
third after being added dropwise
Alkane reaction solution；Filtering adds in 5g sodium hydroxides to
reaction solution, is warming up to 35°C, formaldehyde (40% aqueous
solution) is added dropwise, drip with
the reaction was continued afterwards 3h, obtains 2-Methyl-2-nitropropan-1-ol.
l?uterung methode
Distil it under vacuum and/or crystallise it from pet ether or MeOH. [Astle & Abbott J Org Chem 21 1229 1956, Kambe & Yasuda Bull Soc Chem Jpn 41 1444 1968, Beilstein 1 H 378, 1 III 1546, 1 IV 1604.]
2-Methyl-2-nitropropan-1-ol Upstream-Materialien And Downstream Produkte
Upstream-Materialien
Downstream Produkte
2-Methyl-2-nitropropan-1-ol Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.
Global( 81)Lieferanten
76-39-1(2-Methyl-2-nitropropan-1-ol)Verwandte Suche:
- 2-Nitro-2-methylpropanol
- methyl-2nitro-2propanol
- 2-NITROISOBUTANOL
- Methylnitropropanol
- 2-methyl-2-nitropropan-1-ol
- 2-Methyl-2-nitro-1-propanol>
- 2-methyl-2-nitro-1-propano
- 2-Methyl-2-nitropropanol
- 2-NITRO-2-METHYL-1-PROPANOL
- 2-METHYL-2-NITRO-1-PROPANOL
- 1-Propanol, 2-methyl-2-nitro-
- 76-39-1
- O2NCH32CCH2OH
- O2NCCH32CH2OH
- Building Blocks
- C2 to C6
- Oxygen Compounds
- Organic Building Blocks
- Alcohols
