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Fmoc-Gly-OH

Fmoc-Gly-OH Struktur
29022-11-5
CAS-Nr.
29022-11-5
Englisch Name:
Fmoc-Gly-OH
Synonyma:
FMOC-GLY-OH;FMOC-GLY;FMOC-L-GLY-OH;FMOC-L-GLY;FMOC-GLYCINE;Fmoc-g;Fmoc-GL;Fomc-Gly-OH;FMOC-L-GLYCINE;N-[(9H-FLUOREN-9-YLMETHOXY)CARBONYL]GLYCINE
CBNumber:
CB4288480
Summenformel:
C17H15NO4
Molgewicht:
297.31
MOL-Datei:
29022-11-5.mol

Fmoc-Gly-OH Eigenschaften

Schmelzpunkt:
174-175 °C(lit.)
Siedepunkt:
438.82°C (rough estimate)
Dichte
1.1671 (rough estimate)
Brechungsindex
1.4500 (estimate)
storage temp. 
2-8°C
L?slichkeit
almost transparency in Methanol
pka
3.89±0.10(Predicted)
Aggregatzustand
Powder
Farbe
White
BRN 
2163967
Major Application
peptide synthesis
InChI
InChI=1S/C17H15NO4/c19-16(20)9-18-17(21)22-10-15-13-7-3-1-5-11(13)12-6-2-4-8-14(12)15/h1-8,15H,9-10H2,(H,18,21)(H,19,20)
InChIKey
NDKDFTQNXLHCGO-UHFFFAOYSA-N
SMILES
C(O)(=O)CNC(OCC1C2=C(C=CC=C2)C2=C1C=CC=C2)=O
CAS Datenbank
29022-11-5(CAS DataBase Reference)
Sicherheit
  • Risiko- und Sicherheitserkl?rung
  • Gefahreninformationscode (GHS)
Kennzeichnung gef?hrlicher Xi
R-S?tze: 36/37/38
S-S?tze: 24/25-36-26
WGK Germany  3
HS Code  29242995
Speicherklasse 11 - Combustible Solids
Bildanzeige (GHS) Exclamation Mark (GHS07)
Alarmwort Warnung
Gefahrenhinweise
Code Gefahrenhinweise Gefahrenklasse Abteilung Alarmwort Symbol P-Code
H315 Verursacht Hautreizungen. Hautreizung Kategorie 2 Warnung P264, P280, P302+P352, P321,P332+P313, P362
H319 Verursacht schwere Augenreizung. Schwere Augenreizung Kategorie 2 Warnung P264, P280, P305+P351+P338,P337+P313P
H335 Kann die Atemwege reizen. Spezifische Zielorgan-Toxizit?t (einmalige Exposition) Kategorie 3 (Atemwegsreizung) Warnung
Sicherheit
P261 Einatmen von Staub vermeiden.
P305+P351+P338 BEI KONTAKT MIT DEN AUGEN: Einige Minuten lang behutsam mit Wasser spülen. Eventuell vorhandene Kontaktlinsen nach M?glichkeit entfernen. Weiter spülen.

Fmoc-Gly-OH Chemische Eigenschaften,Einsatz,Produktion Methoden

R-S?tze Betriebsanweisung:

R36/37/38:Reizt die Augen, die Atmungsorgane und die Haut.

S-S?tze Betriebsanweisung:

S24/25:Berührung mit den Augen und der Haut vermeiden.
S36:DE: Bei der Arbeit geeignete Schutzkleidung tragen.
S26:Bei Berührung mit den Augen sofort gründlich mit Wasser abspülen und Arzt konsultieren.

Chemische Eigenschaften

white to light yellow crystal powde

Verwenden

Fmoc-Gly-OH is an N-Fmoc-protected form of Glycine (G615990). Glycine is a nonessential amino acid that acts as an inhibitory neyrotransmitter in the vertebrate central nervous system. Glycine also posesses cytoprotective against oxidant damage in the kidney.

synthetische

Glycine (Gly) (0.5 g, 6.66 mmol) was dissolved in 10% NaCO3 (14 ml) under stirring in a 50-ml flask. To the resulting solution, which had been put into an ice bath, 9-fluorenylmethoxycarbonyl chloride (Fmoc-Cl) (1.72 g, 6.66 mmol) in dioxane (12 ml) was gradually added. The reaction mixture was stirred at room temperature for 4 hours. Then added water (150 ml) to the mixture. The aqueous phase layer was separated from the reaction mixture and stripped with ether three times (75 ml×3). The stripped aqueous layer was acidified with 2N HCl aqueous solution to a pH=2, followed by extraction with ethyl acetate three times (75 ml×3). The organic phase layer was recovered and concentrated to obtain crude product of 1.70 g. The crude product was recrystallized in a mixed solvent of ethyl acetate hexane=1:2 (30 ml), and white solid denoted as Fmoc-Gly-OH was obtained after filtration at a reduced pressure.
Fmoc-Gly-OH

Allgemeine Beschreibung

Fmoc-Gly-OH is used for fmoc solid-phase peptide synthesis.

Fmoc-Gly-OH Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte


Fmoc-Gly-OH Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

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29022-11-5()Verwandte Suche:


  • 9-FLUORENYLMETHOXYCARBONYL-GLYCINE
  • F-FMOC-GLYCINE
  • N-alpha-(9-fluorenylmethyloxycarbonyl)-L-glycine
  • FMOC-Glycine,98%
  • Fmoc-glycine N-(9-Fluorenylmethoxycarbonyl)-glycine
  • N-Fmoc-glycine Fmoc-Gly-OH
  • FMoc-Gly-OH >=98.0% (T)
  • GLYCINE-N-FMOC (13C2,15N)
  • GLYCINE-N-FMOC (13C2,2,2-D2,15N)
  • Fmoc-glycine≥ 99% (HPLC)
  • N-(9-Fluorenylmethoxycarbonyl)-glycine for synthesis
  • npc14692
  • N-ALPHA-FMOC-GLYCINE
  • N-(9-FLUORENYLMETHOXYCARBONYL)-GLYCINE
  • N-9-FMOC-L-GLYCINE
  • N-9-FLUORENYLMETHYLOXYCARBONYLGLYCINE
  • N-ALPHA-(9-FLUORENYLMETHYLOXYCARBONYL)-GLYCINE
  • N-ALPHA-(9-FLUORENYLMETHOXYCARBONYL)-GLYCINE
  • N-FMOC-GLYCINE
  • N-FMOC-L-GLYCINE
  • 2-[(9H-Fluorene-9-yl)methoxycarbonylamino]acetic acid
  • N-[(9H-Fluorene-9-yl)methoxycarbonyl]glycine
  • Glycine-1-13C-N-FMOC
  • Glycine-2-13C-N-FMOC
  • Glycine-UL-13C2,15N-N-FMOC
  • Fmoc-Gly-OH (Fmoc-Glycine)
  • FMOC-GLYCINE-OH
  • glutanmic acid
  • FMOC-L-GLYCINE extrapure
  • Glycine, N-[(9H-fluoren-9-ylmethoxy)carbonyl]-
  • N-(9-Fluorenylmethoxycarbonyl)glycine ,98%
  • (9H-Fluoren-9-yl)MethOxy]Carbonyl Gly-OH
  • FMOC-GLY-OH(29022-11-5)
  • FMOC-Gly-OH 98%
  • N-[(9H-Fluoren-9-ylmethoxy)carbonyl]glycine>
  • FMOC-GLY-OH 25 G
  • FMOC-GLY-OH 100 G
  • FMOC-GLY-OH 250 G
  • FMOC-Glycine USP/EP/BP
  • FMOC-Glycine extrapure, 99%
  • FMOC-GLY-OH
  • FMoc-DL-Glycine
  • N-(fluoren-9-ylmethoxycarbonyl)glycine
  • Fmoc-glycocoll
  • N-Fmoc-glycine, 95%
  • FMOC-L-GLYCINE
  • FMOC-GLYCINE
  • Fmoc-Gly-OH Fmoc-Gly-OH
  • FMOC-L-GLY-OH
  • Fmoc-GL
  • Fmoc-g
  • FMOC-GLY
  • FMOC-L-GLY
  • Fomc-Gly-OH
  • N-[(9H-FLUOREN-9-YLMETHOXY)CARBONYL]GLYCINE
  • 29022-11-5
  • 29011-11-5
  • 26022-11-5
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