2-CHLORO-N-(2-METHOXYPHENYL)ACETAMIDE
- CAS No.
- 55860-22-5
- Chemical Name:
- 2-CHLORO-N-(2-METHOXYPHENYL)ACETAMIDE
- Synonyms
- SKL827;NSC 8284;AKOS B015640;ASISCHEM U00018;AKOS USSH-4110470;AKOS BBS-00003901;ART-CHEM-BB B015640;CHEMBRDG-BB 3015640;2-chloroacetanisidide;2-chloro-o-acetanisidid
- CBNumber:
- CB4113102
- Molecular Formula:
- C9H10ClNO2
- Molecular Weight:
- 199.63
- MDL Number:
- MFCD00095394
- MOL File:
- 55860-22-5.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| 2-CHLORO-2'-METHOXYACETANILIDE Aldrich | S854948 | 50mg | $28.6 |
| 2-chloro-n-(2-methoxyphenyl)acetamide | FC58981 | 500mg | $900 |
| 2-chloro-n-(2-methoxyphenyl)acetamide | FC58981 | 5000mg | $900 |
| 2-chloro-n-(2-methoxyphenyl)acetamide | FC58981 | 2000mg | $900 |
| 2-chloro-n-(2-methoxyphenyl)acetamide | FC58981 | 1000mg | $900 |
| More product size | |||
| Melting point | 51 °C(Solv: ethanol (64-17-5)) |
|---|---|
| Boiling point | 339.0±22.0 °C(Predicted) |
| Density | 1.264±0.06 g/cm3(Predicted) |
| storage temp. | under inert gas (nitrogen or Argon) at 2-8°C |
| pka | 12.27±0.70(Predicted) |
| Appearance | Light brown to brown Solid |
| CAS DataBase Reference | 55860-22-5(CAS DataBase Reference) |
| EWG's Food Scores | 1 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H335 |
| Precautionary statements | P261-P305+P351+P338 |
| Hazard Codes | Xi |
| HazardClass | IRRITANT |
| HS Code | 2924297099 |
2-CHLORO-N-(2-METHOXYPHENYL)ACETAMIDE price More Price(50)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich | S854948 | 2-CHLORO-2'-METHOXYACETANILIDE Aldrich | 55860-22-5 | 50mg | $28.6 | 2023-06-20 | Buy |
| Biosynth | FC58981 | 2-chloro-n-(2-methoxyphenyl)acetamide | 55860-22-5 | 500mg | $900 | 2026-06-04 | Buy |
| Biosynth | FC58981 | 2-chloro-n-(2-methoxyphenyl)acetamide | 55860-22-5 | 5000mg | $900 | 2026-06-04 | Buy |
| Biosynth | FC58981 | 2-chloro-n-(2-methoxyphenyl)acetamide | 55860-22-5 | 2000mg | $900 | 2026-06-04 | Buy |
| Biosynth | FC58981 | 2-chloro-n-(2-methoxyphenyl)acetamide | 55860-22-5 | 1000mg | $900 | 2026-06-04 | Buy |
2-CHLORO-N-(2-METHOXYPHENYL)ACETAMIDE Chemical Properties,Uses,Production
Synthesis
90-04-0
79-04-9
55860-22-5
The general procedure for the synthesis of 2-chloro-N-(2-methoxyphenyl)acetamide from o-methoxyaniline (0.5 g, 4.05 mmol) and chloroacetyl chloride (0.387 mL, 4.87 mmol) was as follows: to a solution of acetonitrile (10.0 mL) of o-methoxyaniline under argon gas protection was added N,N-diisopropyl ethylamine (DIPEA, 1.56 mL 8.93 mmol), followed by slow dropwise addition of chloroacetyl chloride. After the dropwise addition, the reaction mixture was stirred at room temperature for 1 hour. The reaction process was monitored by thin layer chromatography (TLC). After completion of the reaction, the reaction mixture was concentrated and purified by column chromatography (eluent: 20% ethyl acetate/hexane) to afford the target compound 2-chloro-N-(2-methoxyphenyl)acetamide as a brown solid (0.72 g, 89.05% yield). The structure of the product was confirmed by 1H NMR (CDCl3, 400 MHz): δ 8.96 (s, 1H), 8.35 (dd, J = 1.6, 8.0 Hz, 1H), 7.14-7.10 (m, 1H), 7.02-6.97 (m, 1H), 6.94-6.91 (m, 1H), 4.21 (s, 2H), 3.93 (s, 3H).
References
[1] Journal of Medicinal Chemistry, 2017, vol. 60, # 14, p. 6289 - 6304
[2] Bioorganic and Medicinal Chemistry, 2014, vol. 22, # 24, p. 6885 - 6892
[3] Farmaco, 2002, vol. 57, # 3, p. 201 - 206
[4] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006, vol. 45, # 8, p. 1871 - 1879
[5] Bioorganic and Medicinal Chemistry, 2004, vol. 12, # 13, p. 3471 - 3483
2-CHLORO-N-(2-METHOXYPHENYL)ACETAMIDE Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| career henan chemical co | +86-0371-86658258 +8613203830695 | sales@coreychem.com | China | 29815 | 58 |
| CONIER CHEM AND PHARMA LIMITED | +8618523575427 | sales@conier.com | China | 49979 | 58 |
| Dayang Chem (Hangzhou) Co.,Ltd. | +86-0571-88938639 +8617705817739 | info@dycnchem.com | China | 52705 | 58 |
| Labnetwork lnc. | +86-27-50766799 +8618062016861 | contact@labnetwork.com | China | 19987 | 58 |
| PT CHEM GROUP LIMITED | +86-85511178; | peter68@ptchemgroup.com | China | 35425 | 58 |
| GIHI CHEMICALS CO.,LIMITED | +86-571-86217390; +8618058761490 | info@gihichemicals.com | China | 49969 | 58 |
| Jilin Chinese Academy of Sciences-yanshen Technology | +undefined18143011203 | info@chemextension.com | China | 42056 | 58 |
| Aladdin Scientific | tp@aladdinsci.com | United States | 52923 | 58 | |
| Chongqing Chemdad Co., Ltd | +86-023-6139-8061 +86-86-13650506873 | sales@chemdad.com | China | 39927 | 58 |
| NANJING YINGWEN BIOTECHNOLOGY CO LTD | +8613382787392 | sales@aeechem.com | China | 10001 | 58 |
View Lastest Price from 2-CHLORO-N-(2-METHOXYPHENYL)ACETAMIDE manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
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2019-07-06 | 2-Chloro-N-(2-methoxyphenyl)acetamide
55860-22-5
|
$1.00 | 1KG | 98% | 200kg | Career Henan Chemical Co |
-
- 2-Chloro-N-(2-methoxyphenyl)acetamide
55860-22-5
- $1.00
- 98%
- Career Henan Chemical Co
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