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ChemicalBook >> CAS DataBase List >>3-Bromobenzamide

3-Bromobenzamide

CAS No.
22726-00-7
Chemical Name:
3-Bromobenzamide
Synonyms
3-BROMOBENZAMIDE;M-BROMOBENZAMIDE;META-BROMOBENZAMIDE;TIMTEC-BB SBB009893;Benzamide, m-bromo-;Benzamide, 3-bromo-;Bromophenyl formamide;3-(Carbamoyl)bromobenzene
CBNumber:
CB6278007
Molecular Formula:
C7H6BrNO
Molecular Weight:
200.03
MDL Number:
MFCD00017127
MOL File:
22726-00-7.mol
MSDS File:
SDS
Last updated:2026-05-28 05:59:48
Product description Number Pack Size Price
3-Bromobenzamide TMT00344 1 g $586
3-Bromobenzamide >98.0%(HPLC)(N) B5178 5g $39
3-Bromobenzamide >98.0%(HPLC)(N) B5178 25g $121
3-Bromobenzamide 198600 50.00g $130
3-Bromobenzamide 198600 250.00g $552
More product size

3-Bromobenzamide Properties

Melting point 156-159℃
Boiling point 297.4±23.0 °C(Predicted)
Density 1.61
refractive index 1.5500 (estimate)
Flash point 134℃
storage temp. Sealed in dry,Room Temperature
pka 15.38±0.50(Predicted)
form Solid
color White
InChI 1S/C7H6BrNO/c8-6-3-1-2-5(4-6)7(9)10/h1-4H,(H2,9,10)
InChIKey ODJFDWIECLJWSR-UHFFFAOYSA-N
SMILES BrC1=CC(C(N)=O)=CC=C1
CAS DataBase Reference 22726-00-7(CAS DataBase Reference)
FDA UNII 694N917Z7T
UNSPSC Code 12352200
NACRES NA.21

SAFETY

Risk and Safety Statements

Symbol(GHS)  Exclamation Mark (GHS07)
GHS07
Signal word  Warning
Hazard statements  H315-H319-H335
Precautionary statements  P261-P280a-P304+P340-P305+P351+P338-P405-P501a
Hazard Codes  Xi,Xn
Risk Statements  22
WGK Germany  WGK 3
HS Code  29242990
Storage Class 11 - Combustible Solids
Hazard Classifications Acute Tox. 4 Oral
NFPA 704
1
1 0

3-Bromobenzamide price More Price(37)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich TMT00344 3-Bromobenzamide 22726-00-7 1 g $586 2026-04-30 Buy
TCI Chemical B5178 3-Bromobenzamide >98.0%(HPLC)(N) 22726-00-7 5g $39 2026-04-30 Buy
TCI Chemical B5178 3-Bromobenzamide >98.0%(HPLC)(N) 22726-00-7 25g $121 2026-04-30 Buy
Matrix Scientific 198600 3-Bromobenzamide 22726-00-7 50.00g $130 2026-05-18 Buy
Matrix Scientific 198600 3-Bromobenzamide 22726-00-7 250.00g $552 2026-05-18 Buy
Product number Packaging Price Buy
TMT00344 1 g $586 Buy
B5178 5g $39 Buy
B5178 25g $121 Buy
198600 50.00g $130 Buy
198600 250.00g $552 Buy

3-Bromobenzamide Chemical Properties,Uses,Production

Synthesis

3-Bromobenzoic acid

585-76-2

3-Bromobenzamide

22726-00-7

Under argon protection, 820 mg of 3-bromobenzoic acid (4.0 mmol) was suspended in 14 mL of a 6:1 dichloromethane (DCM)/acetonitrile (MeCN) solvent mixture, to which 800 mg of HOBt (4.44 mmol) and 861 mg of EDOHCl (4.4 mmol) were added. After stirring for 10 min, the mixture changed to a clarified solution, which was subsequently cooled to 0 °C in an ice bath. In another round-bottomed flask, 1.64 g NaOH (40 mmol) was added to 2.8 mL of 28% NH4OH solution (20 mmol), and the resulting gaseous NH3 was passed through a NaOH trap and then drummed into the reaction vessel. After stopping the NH3 drumming, the reaction mixture was concentrated under reduced pressure and the residue was dissolved in ethyl acetate (AcOEt, 60 mL) and washed sequentially with 5% KHSO4 (2 × 30 mL), water (20 mL), 5% NaHCO3 (3 × 20 mL) and brine (20 mL). The organic phase was dried with Na2SO4, filtered and evaporated to dryness under reduced pressure to give 700 mg of 3-bromobenzamide in 87% yield.

References

[1] Patent: WO2017/12890, 2017, A1. Location in patent: Page/Page column 28
[2] Phosphorus, Sulfur and Silicon and the Related Elements, 2007, vol. 182, # 3, p. 657 - 666
[3] Tetrahedron Letters, 2005, vol. 46, # 40, p. 6879 - 6882
[4] Journal of Organic Chemistry, 2003, vol. 68, # 16, p. 6431 - 6434
[5] Chemische Berichte, 1871, vol. 4, p. 707

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View Lastest Price from 3-Bromobenzamide manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
3-Bromobenzamide pictures 2026-03-30 3-Bromobenzamide
22726-00-7
1KG 98% 2000 Shenzhen Nexcon Pharmatechs Ltd.
3-Bromobenzamide pictures 2021-11-15 3-Bromobenzamide
22726-00-7
$15.00 1KG 99% 500ton/Month Qiuxian Baitai New Material Co., LTD
3-Bromobenzamide pictures 2019-07-06 3-Bromobenzamide
22726-00-7
$1.00 1G 98% 1000KG Career Henan Chemical Co

3-Bromobenzamide Spectrum

TIMTEC-BB SBB009893 3-BROMOBENZAMIDE META-BROMOBENZAMIDE M-BROMOBENZAMIDE Benzamide, 3-bromo- Benzamide, m-bromo- 3-(Carbamoyl)bromobenzene Bromophenyl formamide 22726-00-7 22728-00-6 Anilines, Amides & Amines Bromine Compounds blocks Bromides Carboxes Aromatics Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts
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