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ChemicalBook >> CAS DataBase List >>N-[5-(2-methoxyethoxy)pyrimidin-2-yl]benzenesulfonamide

N-[5-(2-methoxyethoxy)pyrimidin-2-yl]benzenesulfonamide

CAS No.
339-44-6
Chemical Name:
N-[5-(2-methoxyethoxy)pyrimidin-2-yl]benzenesulfonamide
Synonyms
Glymidine;Glymidinum;Glycodiazin;Glycodiazine;N-[5-(2-methoxyethoxy)pyrimidin-2-yl]benzenesulfonamide;N-[5-(2-methoxyethoxy)-2-pyrimidinyl]benzenesulphonamide;Benzenesulfonamide, N-[5-(2-methoxyethoxy)-2-pyrimidinyl]-
CBNumber:
CB9875258
Molecular Formula:
C13H15N3O4S
Molecular Weight:
309.3409
MDL Number:
MFCD00865503
MOL File:
339-44-6.mol
MSDS File:
SDS
Last updated:2026-05-11 16:31:51
Product description Number Pack Size Price
Glymidine-d5 451373 1mg $523
Glymidine TRC-G752000-2.5MG 2.5mg $55
Glymidine TRC-G752000-10MG 10mg $127
Glymidine TRC-G752000-100MG 100mg $1128
Glymidine G752000 2.5mg $80

N-[5-(2-methoxyethoxy)pyrimidin-2-yl]benzenesulfonamide Properties

Melting point 152-154°
storage temp. Refrigerator
solubility Chloroform (Slightly), Ethyl Acetate (Slightly)
form Solid
color Light Beige
FDA UNII 4C5I4BQZ8F
NCI Drug Dictionary glymidine
ATC code A10BC01

N-[5-(2-methoxyethoxy)pyrimidin-2-yl]benzenesulfonamide price

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Usbiological 451373 Glymidine-d5 339-44-6 1mg $523 2026-06-03 Buy
TRC TRC-G752000-2.5MG Glymidine 339-44-6 2.5mg $55 2026-06-03 Buy
TRC TRC-G752000-10MG Glymidine 339-44-6 10mg $127 2026-06-03 Buy
TRC TRC-G752000-100MG Glymidine 339-44-6 100mg $1128 2026-06-03 Buy
TRC G752000 Glymidine 339-44-6 2.5mg $80 2021-12-16 Buy
Product number Packaging Price Buy
451373 1mg $523 Buy
TRC-G752000-2.5MG 2.5mg $55 Buy
TRC-G752000-10MG 10mg $127 Buy
TRC-G752000-100MG 100mg $1128 Buy
G752000 2.5mg $80 Buy

N-[5-(2-methoxyethoxy)pyrimidin-2-yl]benzenesulfonamide Chemical Properties,Uses,Production

Originator

Redul,Bayer/Schering,W. Germany,1964

Uses

Glymidine is used in biological activities to predict human intestinal absorption in drug discovery.

Definition

ChEBI: Glymidine is a sulfonamide that is N-(pyrimidin-2-yl)benzenesulfonamide which is substituted at position 5 of the pyrimidine ring by a 2-methoxyethoxy group. It is a hypoglycemic drug used for the treatment of diabetes mellitus. It has a role as a hypoglycemic agent. It is a member of pyrimidines, a sulfonamide and a diether. It is a conjugate acid of a glymidine(1-).

Manufacturing Process

210 g phosphorus pentachloride are gradually added to 252 g methoxyethoxyacetaldehyde-di-methoxyethylacetal with agitation. The mixture is externally cooled with ice to hold the reaction temperature below 25°C. Moisture is carefully excluded. After addition of the condensation agent is completed, the reaction mixture is further agitated at room temperature for 30 minutes. 225 ml dimethylformamide are then added drop by drop while the reaction temperature is held at 20°C to 25°C by external cooling of the reaction vessel with ice. When the dimethylformamide has been added, the temperature is raised to 60°C, and this temperature is maintained for 70 minutes.
The temperature is again lowered to 20°C to 25°C and maintained at this value by cooling with ice while 500 ml methanol are added drop by drop. The resulting solution is admixed drop by drop to a suspension of 240 g powdered caustic soda in 800 ml methanol at 20°C to 25°C. After mixing is completed, stirring is continued for 30 minutes at room temperature. The solution now contains inorganic salts and β-dimethylamino-α-methoxyethoxyacrolein.
200 g guanidine nitrate and thereafter 70 g sodium hydroxide are added to the solution. The methanol is evaporated with agitation. The residue is dissolved in 1.5 liters water and is repeatedly extracted with chloroform. The combined chloroform extracts are evaporated to dryness, and the residue is recrystallized from carbon tetrachloride. 80 g of 2-amino-5- methoxyethoxypyrimidine of MP 80°C to 81°C are obtained.
This material is then dissolved in pyridine. Benzenesulfonylchloride is added and the resulting mixture is heated two hours to 60°C. It is then poured into 300 ml water. The precipitate formed thereby is filtered off and dissolved in dilute ammonium hydroxide. The solution is purified with charcoal, and filtered. The filtrate is acidifed with acetic acid to give glymidine.
62 g 2-benzenesulfonamido-5-methoxyethoxypyrimidine are dissolved jointly with 8 g sodium hydroxide in 250 ml ethanol. The solution is evaporated to dryness, and the residue is suspended in 300 ml acetone. The sodium salt of 2-benzenesulfonamido-5-methoxyethoxypyrimidine may be filtered off, washed with acetone, and dried. The yield of glymidine sodium is about 60 g, the MP 220°C to 223°C.

Therapeutic Function

Antidiabetic

N-[5-(2-methoxyethoxy)pyrimidin-2-yl]benzenesulfonamide Preparation Products And Raw materials

N-[5-(2-methoxyethoxy)pyrimidin-2-yl]benzenesulfonamide Suppliers

Global( 19)Suppliers
Supplier Tel Email Country ProdList Advantage
ATK CHEMICAL COMPANY LIMITED
+undefined-21-51877795 ivan@atkchemical.com China 33024 60
TargetMol Chemicals Inc.
+1-781-999-5354; support@targetmol.com United States 39039 58
TargetMol Chemicals Inc.
+17819995354 marketing@targetmol.com United States 19956 58
DAYANG CHEM (HANGZHOU) CO.,LTD
+86-88938639 +86-17705817739 info@dycnchem.com China 53803 58
BOC Sciences 1-631-485-4226; 16314854226 info@bocsci.com United States 9920 65
Shenzhen Polymeri Biochemical Technology Co., Ltd. +86-400-002-6226 +86-13028896684; sales@rrkchem.com China 57422 58
Energy Chemical 021-58432009 400-005-6266 marketing@energy-chemical.com China 44918 58
Ningbo jinuo chemical co., LTD 0574-87314919 057487319282 info@nbinno.com China 7047 58
Chengdu PEIP Pharmaceutical Technology Co., LTD. 028-61715638 18011352545 1242335275@qq.com China 460 58
Shaanxi DIDU pharmaceutical and Chemical Co., Ltd 029-029-81120477 17792793610 1033@dideu.com China 9996 58

View Lastest Price from N-[5-(2-methoxyethoxy)pyrimidin-2-yl]benzenesulfonamide manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
Glymidine pictures 2026-05-11 Glymidine
339-44-6
$1520.00-2500.00 10g TargetMol Chemicals Inc.
  • Glymidine pictures
  • Glymidine
    339-44-6
  • $1520.00-2500.00
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339-44-6(N-[5-(2-methoxyethoxy)pyrimidin-2-yl]benzenesulfonamide)Related Search:

N-[5-(2-methoxyethoxy)pyrimidin-2-yl]benzenesulfonamide N-[5-(2-methoxyethoxy)-2-pyrimidinyl]benzenesulphonamide Glymidine Benzenesulfonamide, N-[5-(2-methoxyethoxy)-2-pyrimidinyl]- Glycodiazin Glycodiazine Glymidinum 339-44-6
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