134-83-8

4-氯二苯氯甲烷(134-83-8)核磁圖(¹³CNMR)

產(chǎn)品名稱:4-氯二苯氯甲烷

CAS:134-83-8

分子式:C13H10Cl2

分子量: 237.12

InChI:InChI=1S/C13H10Cl2/c14-12-8-6-11(7-9-12)13(15)10-4-2-1-3-5-10/h1-9,13H

InChIKey: ALKWTKGPKKAZMN-UHFFFAOYSA-N

Smiles:C1(Cl)=CC=C(C(Cl)C2=CC=CC=C2)C=C1

Mass

MS-NW-8544          
chloro(p-chlorophenyl)phenylmethane
C13H10Cl2           (Mass of molecular ion:    236)

   Source Temperature: 260 °C
   Sample Temperature: 140 °C
   Reservoir, 75 eV

      18.0       1.6
      36.0       5.0
      38.0       2.0
      39.0       5.8
      50.0       4.1
      51.0       6.2
      52.0       1.0
      62.0       3.5
      63.0       8.7
      64.0       1.1
      65.0       2.4
      69.0       1.7
      69.5       6.7
      70.0       1.5
      73.0       1.8
      74.0       3.0
      75.0       4.9
      76.0       2.1
      77.0       3.6
      81.0       3.6
      81.5       7.5
      82.0      20.5
      82.5      18.2
      83.0      12.5
      83.5       1.6
      86.0       2.0
      87.0       3.1
      88.0       1.4
      89.0       5.4
      91.0       1.2
      99.0       2.1
     100.0       2.1
     100.5       1.3
     101.0       1.9
     105.0       3.5
     111.0       1.8
     113.0       2.9
     114.0       1.6
     115.0       4.4
     125.0       1.9
     126.0       1.5
     127.0       1.3
     137.0       1.2
     138.0       1.4
     139.0       8.3
     140.0       1.1
     151.0       1.2
     152.0       2.7
     162.0       1.5
     163.0      10.5
     164.0      11.9
     165.0     100.0
     166.0      74.0
     167.0      20.0
     168.0       2.2
     199.0       3.9
     200.0       1.1
     201.0      97.7
     202.0      17.7
     203.0      31.9
     204.0       5.6
     216.0       1.2
     236.0       1.1

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₃ H₁₀ Cl₂	0.05 ml : 0.5 ml CDCl₃
chloro(p-chlorophenyl)phenylmethane

    Assign.     Shift(ppm)

      A          7.34 to 7.31
      B             7.28
      C             6.047

     Hz     ppm     Int.

    665.00   7.426     26
    662.19   7.394     49
    661.56   7.387     49
    656.00   7.325    327
    654.75   7.311    386
    652.00   7.281   1000
    650.06   7.259    119
    646.94   7.224     52
    645.13   7.204     30
    643.75   7.188     23
    642.88   7.179     24
    541.69   6.049    190

in CDCl3