ChemicalBook CAS DataBase List 1,1,2-Trichloroethane

1,1,2-Trichloroethane synthesis

14synthesis methods

Product Name:1,1,2-Trichloroethane
CAS Number:79-00-5
Molecular formula:C2H3Cl3
Molecular Weight:133.4

First, trichloroethane was put into the reactor, and then trichloroethylene and chlorine gas in 1:1.2 molar ratio were passed at 20~25°℃ for reaction. After water washing and separation, the finished product is obtained. ClCH=CH2+Cl2→Cl2CHCHCl

74-85-1
115 suppliers
$79.00/11l

79-00-5
214 suppliers
$15.00/10 mL

107-06-2 Synthesis

107-06-2
444 suppliers
$14.00/25g

Yield:107-06-2 45 %Chromat. ，79-00-5 35 %Chromat.

Reaction Conditions:

with chlorine at 320;Gas phase;Green chemistry;Reagent/catalyst;Temperature;

Steps:

1.3; 2.3 (3) Catalytic reaction of gas-phase addition of chlorine gas and ethylene
The reactor was heated to 320°C, and 44.8 ml/min of ethylene and 22.4 ml/min of chlorine gas were mixed into the mixing chamber and mixed evenly.After that, it passes through the reactor to the buffer bottle, water washing bottle, concentrated alkali absorber, and cooling collector.After the experiment, the product is mainly distributed in the cooling collector.The collected products were analyzed by GC. The GC results showed that the collected products contained 45% of 1,2-dichloroethane and 35% of 1,1,2-trichloroethane

References:

China Mining Industry University (Beijing);Zhou Biao;Ke Wei;Sun Xukun CN111116304, 2020, A Location in patent:Paragraph 0022; 0024-0026; 0033-0034; 0037-0039; 0046-0047

75-01-4 Synthesis