1,2-BIS-(4-FLUOROPHENYL)ETHANONE synthesis
- Product Name:1,2-BIS-(4-FLUOROPHENYL)ETHANONE
- CAS Number:366-68-7
- Molecular formula:C14H10F2O
- Molecular Weight:232.23
459-56-3
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366-68-7
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$60.00/100 mg
Yield: 74.3%
Reaction Conditions:
with Zn0.6In2S3.6 in acetonitrile at 20; for 15 h;Inert atmosphere;Sealed tube;Irradiation;
Steps:
7 Example 7
In a 5 ml quartz glass reaction tube, 0.2 mmol of 4-fluorobenzyl alcohol was added, and 20 mg of Zn0.6In2S3.6 was weighed to catalyze the reaction, and 1.0 ml of acetonitrile was added thereto, The reaction tube was replaced with argon gas and sealed, and the ambient temperature 6W LED was illuminated for 15 hours. After completion of the reaction, the product was chromatographed, and the mass spectrum showed a molecular weight consistent with 4,4'-difluorodiphenylethanone, and the yield was 74.3%.
References:
Dalian Institute of Chemical Physics;Wang Feng;Luo Nengchao;Wang Min;Hou Tingting;Chi Rihan;Li Hongji;Liu Huifang CN108440259, 2018, A Location in patent:Paragraph 0039; 0040
579-39-5
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366-68-7
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$60.00/100 mg
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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366-68-7
40 suppliers
$60.00/100 mg
462-06-6
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459-04-1
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366-68-7
40 suppliers
$60.00/100 mg
1000210-73-0
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366-68-7
40 suppliers
$60.00/100 mg