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ChemicalBook CAS DataBase List 1,4-Diiodobenzene
624-38-4

1,4-Diiodobenzene synthesis

11synthesis methods
1,4-Diiodobenzene is obtained by diazotising p-iodoaniline followed by substitution. An alternative preparation method involves diazotising p-phenylenediamine hydrochloride, followed by substitution with potassium iodide.
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Yield:624-38-4 95%

Reaction Conditions:

with bis(1,5-cyclooctadiene)nickel (0);cyclopentyl methyl ether;4,4'-di-tert-butyl-2,2'-bipyridine;sodium iodide at 60; for 48 h;Irradiation;Finkelstein Reaction;

References:

Feng, Yunhui;Luo, Hang;Zheng, Wanyao;Matsunaga, Shigeki;Lin, Luqing [ACS Catalysis,2022,vol. 12,# 18,p. 11089 - 11096]

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