1-BROMO-8-PHENYLOCTANE synthesis
- Product Name:1-BROMO-8-PHENYLOCTANE
- CAS Number:54646-75-2
- Molecular formula:C14H21Br
- Molecular Weight:269.22
111-87-5
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558-13-4
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$10.00/1g
54646-75-2
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$45.00/50mg
Yield:-
Reaction Conditions:
with triphenylphosphine in dichloromethane
Steps:
1.a (a)
To an ice cold solution of the octanol (ca. 19.8 mmoles) and carbon tetrabromide (21.98 mmoles) in methylene chloride (50 ml) was added triphenylphosphine (22.30 mmoles) in methylene chloride (50 ml) and the resulting solution was stirred for 2.5 hours. The volatiles were evaporated and the residue was taken up in ether (100 ml), cooled in ice, and filtered. The filtrate was evaporated and distilled to afford 8-phenyloctyl bromide as an oil.
References:
SmithKline Beecham Corporation US4954513, 1990, A
10472-97-6
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54646-75-2
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4549-32-0
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$5.00/1g
591-51-5
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54646-75-2
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4549-32-0
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100-58-3
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$18.00/10ml
54646-75-2
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$45.00/50mg
142-68-7
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$13.00/25mL
54646-75-2
66 suppliers
$45.00/50mg