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ChemicalBook CAS DataBase List 1-BROMOHEXANE-6,6,6-D3
350818-70-1

1-BROMOHEXANE-6,6,6-D3 synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 85 percent / imidazole / dimethylformamide / 1 h / 0 - 20 °C
2: 60 percent / CuCN / tetrahydrofuran / -20 - 20 °C
3: 69 percent / Ph3PBr2 / CH2Cl2 / 0.5 h / 20 °C

References:

Yao, Fen-Mei;Palmer, Sonya L.;Khanolkar, Atmaram D.;Tian, Xiaoyu;Guo, Jianxin;Makriyannis, Alexandros [Journal of labelled compounds and radiopharmaceuticals,2003,vol. 46,# 2,p. 115 - 129]

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