ChemicalBook CAS DataBase List 1-[(chloromethoxy)methyl]-4-methoxybenzene

1-[(chloromethoxy)methyl]-4-methoxybenzene synthesis

3synthesis methods

Product Name:1-[(chloromethoxy)methyl]-4-methoxybenzene
CAS Number:88023-78-3
Molecular formula:C9H11ClO2
Molecular Weight:186.64

1-[(Chloromethoxy)methyl]-4-methoxybenzene is easily prepared from the MTM ether of p-methoxybenzyl alcohol by treatment with Sulfuryl Chloride in CH2Cl2 at -78 °C followed by solvent evaporation and distillation.

88023-83-0 Synthesis

Benzene, 1-Methoxy-4-[[(Methylthio)Methoxy]Methyl]-

88023-83-0
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1-[(chloromethoxy)methyl]-4-methoxybenzene

88023-78-3
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Yield:88023-78-3 80%

Reaction Conditions:

with acetyl chloride in dichloromethane;Inert atmosphere;

References:

Anketell, Matthew J.;Paterson, Ian;Sharrock, Theodore M. [Organic and Biomolecular Chemistry,2020,vol. 18,# 40,p. 8109 - 8118] Location in patent:supporting information

105-13-5
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88023-78-3
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References

Benzenemethanol, 4-methoxy-, sodium salt (1:1)

53942-86-2
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88023-78-3
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References

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1-[(chloromethoxy)methyl]-4-methoxybenzene synthesis