1-METHOXY-4-PHENYLETHYNYL-BENZENE synthesis
14synthesis methods
- Product Name:1-METHOXY-4-PHENYLETHYNYL-BENZENE
- CAS Number:7380-78-1
- Molecular formula:C15H12O
- Molecular Weight:208.26
Yield:7380-78-1 100%
Reaction Conditions:
with copper(l) iodide;1,1'-bis[(5-methyl-2-furanyl)phosphino]ferrocene;potassium carbonate;bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide at 130; for 20 h;Sonogashira cross-coupling;
References:
Hierso, Jean-Cyrille;Fihri, Aziz;Amardeil, Régine;Meunier, Philippe;Doucet, Henri;Santelli, Maurice [Tetrahedron,2005,vol. 61,# 41,p. 9759 - 9766]
