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ChemicalBook CAS DataBase List 1-methylcyclopenta-1,3-diene
96-39-9

1-methylcyclopenta-1,3-diene synthesis

7synthesis methods
1-methylcyclopenta-1,3-diene was prepared by distillation, depolymerize and rectify petroleum pyrolysis tar.
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 90 percent / H2SO4 / 70 °C
2: CH3ONa / methanol / 72 - 100 °C
3: KF-70 / 200 °C

References:

Safarov, M. G.;Bikkulov, R. M.;Safarova, V. G.;Rafikov, S. R. [Bulletin of the Academy of Sciences of the USSR Division of Chemical Science,1982,vol. 31,# 4,p. 789 - 791][Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya,1982,# 4,p. 896 - 899]

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