ChemicalBook CAS DataBase List 1-Propanesulfonyl chloride

1-Propanesulfonyl chloride synthesis

9synthesis methods

Product Name:1-Propanesulfonyl chloride
CAS Number:10147-36-1
Molecular formula:C3H7ClO2S
Molecular Weight:142.6

2,4,6-Trichloro-[1,3,5]-triazine (TCT) was added at room temperature to a solution of propane-1-sulfonic acid in acetone dry, followed by NEt3 dropwise. The resulting mixture was irradiated to 80 °C (50 W of MW power) for 20 min in a sealed tube (10 mL pressure-rated reaction vial) in a self-tuning single-mode irradiating synthesizer. The mixture was cooled rapidly to room temperature by passing compressed air through the microwave cavity for 1 min. After cooling to room temperature, the precipitate was filtered off on Celite to afford 1-Propanesulfonyl chloride[1].

629-19-6
328 suppliers
$13.00/5g

10147-36-1
219 suppliers
$5.00/5g

Yield:10147-36-1 98%

Reaction Conditions:

with chloro-trimethyl-silane;potassium nitrate in dichloromethane at 50; for 4 h;

References:

Prakash, G. K. Surya;Mathew, Thomas;Panja, Chiradeep;Olah, George A. [Journal of Organic Chemistry,2007,vol. 72,# 15,p. 5847 - 5850]

5284-66-2 Synthesis

5284-66-2
104 suppliers
$76.00/1g

10147-36-1
219 suppliers
$5.00/5g

References

4253-91-2 Synthesis

4253-91-2
28 suppliers
inquiry

10147-36-1
219 suppliers
$5.00/5g

References

4251-16-5
26 suppliers
inquiry

10147-36-1
219 suppliers
$5.00/5g

References

14533-63-2
163 suppliers
$33.00/1g

10147-36-1
219 suppliers
$5.00/5g

References

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1-Propanesulfonyl chloride synthesis

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