1-[3,4-dihydroxy-5-(hydroxymethyl)oxolan-2-yl]-4-(hydroxyamino)pyrimidin-2-one synthesis
- Product Name:1-[3,4-dihydroxy-5-(hydroxymethyl)oxolan-2-yl]-4-(hydroxyamino)pyrimidin-2-one
- CAS Number:13491-41-3
- Molecular formula:C9H13N3O6
- Molecular Weight:259.216
3083-77-0
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13491-41-3
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: dmap; 1H-imidazole / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere
1.2: 16 h / 20 °C
2.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere
3.1: hydroxylamine hydrochloride; triethylamine / acetonitrile / 16 h / 0 - 20 °C / Inert atmosphere
4.1: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 96 h / 20 °C / Inert atmosphere
References:
WO2016/106050,2016,A1
82855-62-7
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13491-41-3
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