2,2,2-Trifluoroethyl methacrylate synthesis
- Product Name:2,2,2-Trifluoroethyl methacrylate
- CAS Number:352-87-4
- Molecular formula:C6H7F3O2
- Molecular Weight:168.11
Yield:352-87-4 33.9 g
Reaction Conditions:
with 1-methyl-1H-imidazole at 20; for 4 h;
Steps:
1 Production Example 1
15.0 g of 2,2,2-trifluoroethanol and 9.8 g of 1-methylimidazole were placed in a glass reaction vessel, and 10.5 g of methacrylic acid chloride was added dropwise at room temperature and stirred for 4 hours. After the completion of the reaction, the product liquid was 33.9 g, and as a result of analyzing this reaction product solution,The reaction product liquid is methacrylic acid15.8 g of 2,2,2-trifluoroethyl ester as an ionic liquidIt contained 11.1 g of 1-methylimidazole hydrochloride
References:
DAIKIN INDUSTRIES LIMITED;GOTO, AKIHIRO;KISHIKAWA, YOSUKE;NAMIKAWA, TAKASHI;MIYAZAKI, MANAHO JP2017/36231, 2017, A Location in patent:Paragraph 0066
