Acetonitrile synthesis
- Product Name:Acetonitrile
- CAS Number:75-05-8
- Molecular formula:C2H3N
- Molecular Weight:41.05
75-07-0
431 suppliers
$14.00/5mL
75-05-8
1057 suppliers
$10.00/10g
Yield:75-05-8 100%
Reaction Conditions:
with N-(4-sulphonic acid)butylpyridinium hydrogen sulphate;C9H13NO3S*2H3NO*H(1+)*HO4S(1-) in para-xylene at 120; under 760.051 Torr; for 2 h;Catalytic behavior;Green chemistry;Temperature;Time;
Steps:
1-6 Example 1
Acetaldehyde (3.6 mmol),1-sulfobutylpyridine hydrogensulfate ionic liquid hydroxylamine salt (5.4mmol)Add to a 100 mL three-necked flask,Add 4mL 1-sulfobutylpyridine hydrogensulfate ionic liquid and 8 mL of p-xylene, stirred,Reflux condensation, at atmospheric pressure,The reaction was stopped after reacting at 120 ° C for 2 h.The reaction solution was cooled to room temperature.Take the supernatant directly into the gas chromatographLine analysis,The result of the reaction is that the conversion of acetaldehyde is 100%.The yield of acetonitrile was 100%.
References:
CN109748817,2019,A Location in patent:Paragraph 0027-0038
64-19-7
1679 suppliers
$10.00/25ML
75-05-8
1057 suppliers
$10.00/10g
107-29-9
223 suppliers
$9.00/1g
75-05-8
1057 suppliers
$10.00/10g
64-17-5
856 suppliers
$10.00/50g
75-05-8
1057 suppliers
$10.00/10g
631-61-8
839 suppliers
$11.19/100G
75-05-8
1057 suppliers
$10.00/10g