ChemicalBook CAS DataBase List Trimethylsilyl cyanide

Trimethylsilyl cyanide synthesis

13synthesis methods

Product Name:Trimethylsilyl cyanide
CAS Number:7677-24-9
Molecular formula:C4H9NSi
Molecular Weight:99.21

Trimethylsilyl cyanide, (CH3)3 Si-CN, is obtained by reacting trimethylsilyl chloride with an approximately equimolar amount of an alkali metal cyanide in the absence of water and in the presence of catalytic, sub-stoichiometric amounts of both an alkali metal iodide and N-methylpyrrolidone, at a temperature of from 15°-25° C.
Trimethylsilyl cyanide is very toxic. All reactions in this sequence should be carried out in a hood.
Preparation of trimethylsilyl cyanide
TRIMETHYLSILYL CYANIDE: CYANOSILATION OF p-BENZOQUINONE

18306-29-1 Synthesis

18306-29-1
117 suppliers
$13.00/5g

151-50-8
0 suppliers
$47.79/100g

7677-24-9
392 suppliers
$19.00/5g

Yield:7677-24-9 96%

Reaction Conditions:

with 1-methyl-pyrrolidin-2-one at 200;

References:

Kantlehner, Willi;Haug, Erwin;Mergen, Walter W. [Synthesis,1980,# 6,p. 460 - 461]

75-77-4
590 suppliers
$5.04/10

151-50-8
0 suppliers
$47.79/100g

7677-24-9
392 suppliers
$19.00/5g

References

75-77-4
590 suppliers
$5.04/10

143-33-9 Synthesis

143-33-9
0 suppliers
$10.00/1g

7677-24-9
392 suppliers
$19.00/5g

References

3012-37-1
131 suppliers
$14.00/1g

81290-20-2 Synthesis

81290-20-2
427 suppliers
$13.00/1g

7677-24-9
392 suppliers
$19.00/5g

351-60-0
40 suppliers
$52.00/5g

References

19942-78-0
22 suppliers
inquiry

81290-20-2 Synthesis

81290-20-2
427 suppliers
$13.00/1g

7677-24-9
392 suppliers
$19.00/5g

134776-65-1
1 suppliers
inquiry

References

Trimethylsilyl cyanide Related Search:

(Trifluoromethyl)trimethylsilane TRIMETHYLSILANE Phosphonitrilic chloride trimer Tosylmethyl isocyanide tert-Butyldimethylsilyl chloride PHENYLTRIMETHYLSILANE Trimethylsilyl trifluoromethanesulfonate Trimethoxysilane Trimethyl thiazole Trimethoxysilylpropanethiol

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Trimethylsilyl cyanide synthesis

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