2',2,2-TRIMETHYLPROPIOPHENONE synthesis
- Product Name:2',2,2-TRIMETHYLPROPIOPHENONE
- CAS Number:2041-37-4
- Molecular formula:C12H16O
- Molecular Weight:176.25
938-16-9
89 suppliers
$14.00/100mg
75-24-1
172 suppliers
$54.50/100ml
2041-37-4
34 suppliers
$27.00/250mg
Yield:2041-37-4 98%
Reaction Conditions:
Stage #1: 2,2-dimethylpropiophenone;trimethylaluminumwith iron(III)-acetylacetonate;4-(bis(2-(diphenylphosphanyl)phenyl)phosphanyl)-N,N-dimethylaniline in tetrahydrofuran;toluene at 20;Inert atmosphere;Schlenk technique;
Stage #2: with 2,3-dichlorobutane in tetrahydrofuran;toluene at 70; for 16 h;Mechanism;Inert atmosphere;Schlenk technique;Sealed tube;
References:
Shang, Rui;Ilies, Laurean;Nakamura, Eiichi [Journal of the American Chemical Society,2016,vol. 138,# 32,p. 10132 - 10135] Location in patent:supporting information
22526-24-5
16 suppliers
$200.00/100mg
66423-62-9
12 suppliers
inquiry
2041-37-4
34 suppliers
$27.00/250mg
95-46-5
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$10.00/10g
3282-30-2
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$19.85/100ml
2041-37-4
34 suppliers
$27.00/250mg
55678-42-7
1 suppliers
inquiry
2041-37-4
34 suppliers
$27.00/250mg
3282-30-2
373 suppliers
$19.85/100ml
108-88-3
0 suppliers
$14.00/100ml
2041-37-4
34 suppliers
$27.00/250mg
98-51-1
238 suppliers
$10.00/1g
30314-44-4
45 suppliers
$24.00/100mg