4-tert-Butyltoluene synthesis
- Product Name:4-tert-Butyltoluene
- CAS Number:98-51-1
- Molecular formula:C11H16
- Molecular Weight:148.24
877-65-6
198 suppliers
$41.89/5g
98-51-1
242 suppliers
$10.00/1g
Yield:98-51-1 90 %Chromat.
Reaction Conditions:
with triethylsilane in ethanol at 20; for 0.166667 h;Inert atmosphere;
Steps:
2.4. General procedure for benzyl alcohol hydrogenolysis
General procedure: To a solution of benzyl alcohol (1mmol) and triethylsilane (amountindicated in Table 2) in ethanol (5mL)was added 10 mg of Pd NPs/rGO under an argon atmosphere. The resulting mixture was stirred for thetime indicated in Table 2 prior to GC-MS analysis. The resultingmixturewas filtered and washed by ethyl acetate for catalyst separation. Thepure product in entry 1 was isolated by distillation; for entries 2-10the products were isolated by column chromatography using hexane/ethyl acetate (9/1) as eluent.
References:
Mirza-Aghayan, Maryam;Molaee Tavana, Mahdieh;Boukherroub, Rabah [Catalysis Communications,2015,vol. 69,p. 97 - 103]
49543-63-7
153 suppliers
$9.00/25g
98-51-1
242 suppliers
$10.00/1g
18880-00-7
222 suppliers
$9.00/5g
98-51-1
242 suppliers
$10.00/1g
108-88-3
0 suppliers
$21.80/5 mL
75-65-0
795 suppliers
$10.00/10ml
98-51-1
242 suppliers
$10.00/1g
15181-11-0
124 suppliers
$23.00/5g
1075-38-3
58 suppliers
$141.00/1g
