2,5-dichloroanilinium chloride synthesis
- Product Name:2,5-dichloroanilinium chloride
- CAS Number:33663-41-1
- Molecular formula:C6H6Cl3N
- Molecular Weight:198.4775
33663-41-1
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68-11-1
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$12.00/25g
6274-27-7
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$17.67/250mgs:
Yield:6274-27-7 54%
Reaction Conditions:
Stage #1: 2,5-dichloroaniline hydrochloridewith sodium nitrite at 10; for 1 h;Diazotization;
Stage #2: mercaptoacetic acidwith hydrogenchloride;copper(II) sulfate at 20 - 50;Substitution;
References:
D'Andrea, Stan V.;Bonner, Daniel;Bronson, Joanne J.;Clark, Junius;Denbleyker, Ken;Fung-Tomc, Joan;Hoeft, Shelley E.;Hudyma, Thomas W.;Matiskella, John D.;Miller, Raymond F.;Misco, Peter F.;Pucci, Michael;Sterzycki, Roman;Tsai, Yuan;Ueda, Yasutsuga;Wichtowski, John A.;Singh, Janak;Kissick, Thomas P.;North, Jeffery T.;Pullockaran, Annie;Humora, Michael;Boyhan, Brenda;Vu, Truc;Fritz, Alan;Heikes;Fox, Rita;Godfrey, Jollie D.;Perrone, Robert;Kaplan, Murray;Kronenthal, David;Mueller, Richard H. [Tetrahedron,2000,vol. 56,# 31,p. 5687 - 5698]
33663-41-1
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13201-85-9
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33663-41-1
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![2-[(2,5-Dichlorophenyl)thio]acetyl chloride](/CAS/20210305/GIF/57833-03-1.gif)
57833-03-1
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