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ChemicalBook CAS DataBase List 2,6-DIMETHYL-4'-METHOXYBENZOPHENONE
52629-41-1

2,6-DIMETHYL-4'-METHOXYBENZOPHENONE synthesis

2synthesis methods
608-28-6 Synthesis
2-Iodo-1,3-dimethylbenzene

608-28-6
186 suppliers
$9.00/1g

201230-82-2 Synthesis
carbon monoxide

201230-82-2
1 suppliers
inquiry

5720-07-0 Synthesis
4-Methoxyphenylboronic acid

5720-07-0
469 suppliers
$6.00/5g

-

Yield:52629-41-1 99%

Reaction Conditions:

with [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(II) dichloride;caesium carbonate in 1,4-dioxane at 140; under 3102.97 Torr; for 24 h;Inert atmosphere;

References:

Michael O'Keefe;Simmons, Nicholas;Martin, Stephen F. [Organic Letters,2008,vol. 10,# 22,p. 5301 - 5304] Location in patent:supporting information; experimental part

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