2-(ALLYLDIMETHYLSILYL)PYRIDINE synthesis
- Product Name:2-(ALLYLDIMETHYLSILYL)PYRIDINE
- CAS Number:118722-54-6
- Molecular formula:C10H15NSi
- Molecular Weight:177.32
109-04-6
527 suppliers
$6.00/25g
4028-23-3
115 suppliers
$30.00/1g
118722-54-6
32 suppliers
$165.00/1g
Yield:118722-54-6 76%
Reaction Conditions:
Stage #1: 2-bromo-pyridinewith n-butyllithium in hexane at -78; for 1 h;Inert atmosphere;Schlenk technique;
Stage #2: Allylchlorodimethylsilane in hexane at -78 - 20; for 18 h;Inert atmosphere;Schlenk technique;
References:
Frogneux, Xavier;Von Wolff, Niklas;Thuéry, Pierre;Lefèvre, Guillaume;Cantat, Thibault [Chemistry - A European Journal,2016,vol. 22,# 9,p. 2930 - 2934] Location in patent:supporting information