ChemicalBook CAS DataBase List 2-(Trimethylsilyl)pyridine

2-(Trimethylsilyl)pyridine synthesis

4synthesis methods

Product Name:2-(Trimethylsilyl)pyridine
CAS Number:13737-04-7
Molecular formula:C8H13NSi
Molecular Weight:151.28

A solution of 2-chloropyridine (20.7 mL, 217 mmol) and trimethylchlorosilane (28.0 mL, 221 mmol) in THF (100 mL) was added dropwise to a rapidly stirred mixture of magnesium chips (6.75 g, 281 mmol) in THF (175 mL). The solution in was added dropwise to

110-86-1 Synthesis

110-86-1
890 suppliers
$9.00/5g

75-77-4
588 suppliers
$5.04/10

13737-04-7
165 suppliers
$20.00/1g

Yield: 80%

Reaction Conditions:

with n-butyllithium;2-(N,N-dimethylamino)ethanol1.) hexane, -78 deg C, 1 h, 2.) THF, -78 deg C, 1 h;

References:

Gros, Philippe;Fort, Yves;Caubere, Paul [Journal of the Chemical Society. Perkin transactions I,1997,# 24,p. 3597 - 3600]

109-04-6 Synthesis

109-04-6
527 suppliers
$6.00/25g

75-77-4
588 suppliers
$5.04/10

13737-04-7
165 suppliers
$20.00/1g

References

109-09-1
0 suppliers
$10.60/1gm:

75-77-4
588 suppliers
$5.04/10

13737-04-7
165 suppliers
$20.00/1g

References

110-86-1 Synthesis

110-86-1
890 suppliers
$9.00/5g

75-77-4
588 suppliers
$5.04/10

13737-04-7
165 suppliers
$20.00/1g

17379-37-2
19 suppliers
inquiry

18301-46-7
21 suppliers
inquiry

References

2-(Trimethylsilyl)pyridine Related Search:

Benzyltrimethylammonium chloride 2-Chloro-5-(chloromethyl)pyridine Trimethylamine hydrochloride Pyridine 2,3,5-Collidine 2,6-Lutidine Vinyltrimethoxysilane 2,4,6-Collidine 3-FLUORO-2-TRIMETHYLSILANYL-PYRIDINE 3-Chloro-2-(trimethylsilyl)pyridine

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2-(Trimethylsilyl)pyridine synthesis

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