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ChemicalBook CAS DataBase List 2-Bromofluorobenzene
1072-85-1

2-Bromofluorobenzene synthesis

10synthesis methods
NaOMe (0.5 mmol; 25 wt% MeOH solution) was added to a slurry of arylboronic acid (10 mmol) in acetonitrile (10 mL/g vs. boric acid). One portion of 1,3-dibromo-5,5-dimethylglycolide (11 mmol) was added to the reaction and the mixture was heated to 40 °C.
-

Yield:1072-85-1 90%

Steps:

6 Example 6

Example 6 The procedure as for Example 1 was followed, but in place of the aniline, 1.72 parts of bromoaniline were used. Decomposition started at 105°C, heating was continued up to 160°C and 2-bromofluorobenzene (90%) was obtained.

References:

EP430434,1991,A2

2-Bromofluorobenzene Related Search:

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