2-(Bromomethyl)pyridine synthesis
- Product Name:2-(Bromomethyl)pyridine
- CAS Number:55401-97-3
- Molecular formula:C6H6BrN
- Molecular Weight:172.02
31106-82-8
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Yield:55401-97-3 100%
Reaction Conditions:
with potassium carbonate in acetone at 25; for 7 h;
Steps:
L1.2
Step 2; 760 mg (3 mmol) of 2-bromomethylpyridine.HBr and 436 mg (3.15 mmol) of potassium carbonate were degassed under vacuum for 1 hour. 10 ml_ of dry acetone were added and the mixture was stirred under argon for 6 hours at room temperature (about 25 0C). The solvent was removed and the 2-bromomethylpyhdine was extracted with 3 x 10 ml_ of diethyl ether under inert atmosphere. The solvent was removed to afford a pink oil with quantitative yield.
References:
TOTAL PETROCHEMICALS RESEARCH FELUY WO2008/61900, 2008, A1 Location in patent:Page/Page column 8
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