2-CHLORO-4'-METHOXYBENZOPHENONE synthesis
- Product Name:2-CHLORO-4'-METHOXYBENZOPHENONE
- CAS Number:54118-74-0
- Molecular formula:C14H11ClO2
- Molecular Weight:246.69
609-65-4
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100-66-3
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54118-74-0
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Yield:54118-74-0 98%
Reaction Conditions:
with copper(II) ferrite in 1,2-dichloro-ethane at 35 - 38; for 18 h;Friedel-Crafts Acylation;
Steps:
General procedure: The FC acylation of various benzenes with acid chlorides was carried out in the presence of magnetic nano CuFe2O4 (particle size = 50 nm) by using one of the reaction condition (A-D) given below. Condition A: Anisole/arene (1 mmol), acid chloride (1.2 mmol), nano CuFe2O4 (20 mol %), 1,2-DCE (2 mL), 80 C and 24 h. Condition B: Anisole/arene (1 mmol), acid chloride (1.2 mmol), nano CuFe2O4 (20 mol %), 1,2-DCE (2 mL), rt (35-38 C) and 18 h. Condition C: Neat reaction, anisole/arene (3.3 mmol), acid chloride (1.2 mmol), nano CuFe2O4 (20 mol %), rt (35-38 C) and 18 h. Condition D: Neat reaction, arene/anisole (3.3 mmol), acid chloride (1.2 mmol), nano CuFe2O4 (20 mol %), 80 C and 18 h.
References:
Parella, Ramarao;Naveen;Kumar, Amit;Babu, Srinivasarao Arulananda [Tetrahedron Letters,2013,vol. 54,# 13,p. 1738 - 1742] Location in patent:supporting information
![Benzene, 1-chloro-2-[(4-methoxyphenyl)methyl]-](/CAS/20210305/GIF/53039-46-6.gif)
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54118-74-0
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123-11-5
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54118-74-0
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118-91-2
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54118-74-0
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