2-Chloro-4-nitroaniline synthesis
- Product Name:2-Chloro-4-nitroaniline
- CAS Number:121-87-9
- Molecular formula:C6H5ClN2O2
- Molecular Weight:172.57
99-54-7
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$13.00/25g
121-87-9
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$35.79/250g
Yield:121-87-9 99.45%
Reaction Conditions:
with ammonium hydroxide;tetrabutylammomium bromide;copper(l) chloride in water at 140; under 24002.4 Torr;Reagent/catalyst;Temperature;Pressure;
Steps:
1.c; 2.c; 3.c; 1.c; 2.c; 3.c; 4.c; 5-10
(c) Aminolysis reaction: add 150g of high-purity 3,4-dichloronitrobenzene prepared in step to 200g of water, addCuprous chloride 1.5g, tetrabutyl bromide press 3.5g, lead to the recovery of 65g of the previous batch of ammonia, then add 60g of liquid ammonia, and raise the temperature to 140C, the pressure is 3.2 MPa, the heat preservation reaction is to the end, cooling and washing, to obtain 134 g of o-chloro-p-nitroaniline, purity 99.2%.
References:
Zhejiang Runtu Institute Co., Ltd.;Gu Gaowei;Chen Baoxing;Gao Lijiang;Huang Zhong CN111039798, 2020, A Location in patent:Paragraph 0040; 0043; 0046; 0049; 0051; 0054; 0056; 0059
100-01-6
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121-87-9
38 suppliers
$35.79/250g
121-73-3
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$10.00/1g
121-87-9
38 suppliers
$35.79/250g
121-73-3
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$10.00/1g
769-11-9
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89-63-4
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$13.00/50g
121-87-9
38 suppliers
$35.79/250g