ChemicalBook CAS DataBase List 2-Deoxy-D-glucose

2-Deoxy-D-glucose synthesis

9synthesis methods

Product Name:2-Deoxy-D-glucose
CAS Number:154-17-6
Molecular formula:C6H12O5
Molecular Weight:164.16

The synthesis of 2-deoxy-D-glucose comprising haloalkoxylation of R-D-Glucal wherein R is selected from H and 3, 4, 6-tri-O-benzyl, to obtain alkyl 2-deoxy-2-halo-R-α/β-D-gluco/mannopyranoside, converting alkyl 2-deoxy-2-halo-R-α/β-D-gluco/mannopyranoside by reduction to alkyl 2-deoxy-α/β-D-glucopyranoside, hydrolysing alkyl 2-deoxy-α/β-D-glucopyranoside to 2-deoxy-D-glucose.

D-threo-Hexos-5-ulose, cyclic 1-(1,3-propanediyl acetal) (9CI)

124266-48-4
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154-17-6
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1.) NaHB(OAc)3, 2.) L-iditol dehydrogenase, triosephosphate isomerase, NAD⁽¹⁺⁾, L-glutamic dehydrogenase, 2-ketoglutarate, ammonium sulfate / acetic acid
2: 95 percent / 1.0 M aq. HCl / tetrahydrofuran

References:

Borysenko;Spaltenstein;Straub;Whitesides [Journal of the American Chemical Society,1989,vol. 111,# 26,p. 9275 - 9276]

D-arabino-Hexose, 2-deoxy-, cyclic 1,3-propanediyl acetal (9CI)

124266-10-0
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154-17-6
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References

D-arabino-Heptose, 2,3-dideoxy-4,5:6,7-bis-O-(1-methylethylidene)-

149180-91-6
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154-17-6
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References

D-arabino-Hexose, 2-deoxy-4,5-O-(1-methylethylidene)-, dimethyl acetal (9CI)

73982-69-1
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154-17-6
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References

β-D-arabino-Hexopyranoside, [(1S,4aS,6S,7S,7aS)-1,4a,5,6,7,7a-hexahydro-6-hydroxy-7-(hydroxymethyl)-1-(3-methyl-1-oxobutoxy)cyclopenta[c]pyran-4-yl]methyl 2-deoxy-

1187828-71-2
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154-17-6
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$6.00/250mg

References

2-Deoxy-D-glucose Related Search:

Desogestrel D(+)-Glucose Chenodeoxycholic acid Ursodeoxycholic acid D-(-)-Salicin Maltitol 6-FLUORO-6-DEOXY-D-GLUCOPYRANOSE 6-Amino-6-deoxy-D-glucopyranose, hydrochloride KANOSAMINE, HYDROCHLORIDE 3-DEOXY-3-FLUORO-D-GLUCOSE

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2-Deoxy-D-glucose synthesis

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