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ChemicalBook CAS DataBase List 2-dimethylaminophenol
3743-22-4

2-dimethylaminophenol synthesis

12synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 23 °C / Inert atmosphere
2.1: trifluoroacetic anhydride / dichloromethane / 1 h / -78 °C / Inert atmosphere
2.2: 0.25 h / -78 - 0 °C / Inert atmosphere

References:

Lewis, Robert S.;Wisthoff, Michael F.;Grissmerson;Chain, William J. [Organic Letters,2014,vol. 16,# 14,p. 3832 - 3835]

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