2-ethylhexyl oleate synthesis
- Product Name:2-ethylhexyl oleate
- CAS Number:26399-02-0
- Molecular formula:C26H50O2
- Molecular Weight:394.67
Yield: 96%
Reaction Conditions:
with porous phenol sulfonic acid-formaldehyde resin in neat (no solvent) at 90; for 6 h;
Steps:
General Esterification Procedure
General procedure: The esterification reaction was carried out in a 20 mL glass vialwith a magnetic bar. Oleic acid (10 mmol), alcohol substrate (12mmol), and PSF catalyst (1.4 mol%) were added at 90 °C. Thereaction mixture was analyzed by diluting a sample 5 timeswith heptane using an internal standard (methyl heptadecanoate),and analyzed via gas chromatography (GC) and massspectrometry (GC-MS). After reaction was complete, the catalystwas separated from the reaction products by filtration andwas dried in vacuo.
References:
Kim, Yo-Han;Han, Jusung;Jung, Byeong Yeon;Baek, Heeyoel;Yamada, Yoichi M. A.;Uozumi, Yasuhiro;Lee, Yoon-Sik [Synlett,2016,vol. 27,# 1,art. no. ST-2015-D0448-L,p. 29 - 32] Location in patent:supporting information
