2-HYDROXY-5-IODO-BENZONITRILE synthesis
- Product Name:2-HYDROXY-5-IODO-BENZONITRILE
- CAS Number:685103-95-1
- Molecular formula:C7H4INO
- Molecular Weight:245.02
(1)Synthesis of 5-iodo-2-hydroxybenzaldehyde oxime
Add 30g 5-iodo-2-hydroxybenzaldehyde to 270ml ethanol, dropwise add 17g hydroxylamine hydrochloride, room temperature stirring overnight, cooling, add water and ethyl acetate, extraction and part
2314-30-9
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Yield:685103-95-1 92%
Reaction Conditions:
with 4-methyl-morpholine for 5 h;Heating;
References:
Talekar, Rahul Subhash;Chen, Grace Shiahuy;Lai, Shin-Yu;Chern, Ji-Wang [Journal of Organic Chemistry,2005,vol. 70,# 21,p. 8590 - 8593]
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