ChemicalBook CAS DataBase List 2-Methoxybenzyl alcohol

2-Methoxybenzyl alcohol synthesis

11synthesis methods

Product Name:2-Methoxybenzyl alcohol
CAS Number:612-16-8
Molecular formula:C8H10O2
Molecular Weight:138.16

Synthesis of 2-Methoxybenzyl Alcohol: Under an inert nitrogen (N?) atmosphere, after dehydration and deoxygenation, 2-methoxybenzoic acid (76.2 mg, 0.5 mmol) was added to the reaction flask, followed by the addition of liquid borane (290 μL, 2 mmol). The reaction was carried out at room temperature for 12 hours. After completion, the mixture was removed from the glovebox, and trimethoxybenzene (84.23 mg, 0.5 mmol) was added as an internal standard. The mixture was dissolved in CDCl?, stirred for 10 minutes, and then sampled for nuclear magnetic resonance (NMR) analysis. The yield was calculated to be 99%.

135-02-4
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612-16-8
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Yield:612-16-8 100%

Reaction Conditions:

with sodium tetrahydroborate in methanol at 20; for 1 h;

Steps:

Step-I (Preparation of benzyl alcohols)
General procedure: benzaldehyde derivatives (1 mmol) in methanol (15 mL), sodium borohydride (2 mmol) and stirred at room temperature for 1 h. Usual work-up, quantitative yield.

References:

Parihar, Swati;Kumar, Amit;Chaturvedi, Amit K.;Sachan, Naresh Kumar;Luqman, Suaib;Changkija, Bendangla;Manohar, Murli;Prakash, Om;Chanda;Khan, Feroz;Chanotiya;Shanker, Karuna;Dwivedi, Anila;Konwar, Rituraj;Negi, Arvind S. [Journal of Steroid Biochemistry and Molecular Biology,2013,vol. 137,p. 332 - 344]

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579-75-9 Synthesis

579-75-9
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612-16-8
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References

6850-57-3
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612-16-8
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References

606-45-1 Synthesis

606-45-1
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612-16-8
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References

Benzene, 1-methoxy-2-[[(trimethylsilyl)oxy]methyl]-

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612-16-8
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References

2-Methoxybenzyl alcohol Related Search:

Ethyl acetate 4-Hydroxybenzyl alcohol Benzyl alcohol Triphenylmethanol 4-Methylbenzyl alcohol Benzhydrol 3-Phenoxybenzyl alcohol 2,6-Dimethoxybenzoic acid 2,4,5-Trimethoxybenzoic acid 2,4-Dimethoxybenzoic acid

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2-Methoxybenzyl alcohol synthesis

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