2-Nonanone synthesis
- Product Name:2-Nonanone
- CAS Number:821-55-6
- Molecular formula:C9H18O
- Molecular Weight:142.24
29214-60-6
100 suppliers
$126.00/500mg
821-55-6
338 suppliers
$7.00/25g
Yield:821-55-6 1 g
Reaction Conditions:
with water;sodium hydroxide at 20; for 5 h;
Steps:
19.B B) Preparation of nonan-2-one
A solution of 2-acetyl-octanoic acid ethyl ester (4.0 g, 18.6 mmol) in 5% aqueous NaOH solution (22.6 ml) was allowed to stir for 5 h at RT. The reaction was monitored by TLC and after completion of the reaction, mixture was acidified with 50 % H2S04 (pH = 2). Then themixture was concentrated until mass becomes half, cooled the reaction mixture to 0 °C. To this mixture saturated K2C03 solution was added and the mixture was subjected to a standard ether work up to give 1.0 g of the desired product as a liquid, which was used for the next step without purification.
References:
F2G LIMITED;SIBLEY, Graham Edward Morris;MALMSTR?M, Lars Jonas;LARSSON, Johanna Maria WO2017/9651, 2017, A1 Location in patent:Page/Page column 56
14309-57-0
117 suppliers
$18.89/10g
821-55-6
338 suppliers
$7.00/25g
124-11-8
125 suppliers
$45.00/250mg
821-55-6
338 suppliers
$7.00/25g
628-99-9
142 suppliers
$27.00/5mL
821-55-6
338 suppliers
$7.00/25g
18402-83-0
65 suppliers
$24.00/5g
821-55-6
338 suppliers
$7.00/25g