2-Propen-1-ol, 2-methyl-, 1-formate synthesis
- Product Name:2-Propen-1-ol, 2-methyl-, 1-formate
- CAS Number:820-57-5
- Molecular formula:C5H8O2
- Molecular Weight:100.12
Yield:820-57-5 96%
Reaction Conditions:
with copper dichloride;ascorbic acid in water; for 4 h;Reflux;Reagent/catalyst;
Steps:
1-2 Example 2
In the reaction kettle, add 2000g of methallyl chloride, add 1600g of sodium formate, add 500g of water, and add 50g of copper chloride. 700g of 19% vitamin C aqueous solution was added dropwise, and the reaction temperature was controlled under reflux. After 4 hours of reaction, the gas phase was detected and the reaction was basically over. The content of each component was 0.2% of raw material methallyl chloride, 96% of methallyl formate, 3.5% of methallyl alcohol, and methallyl ether. 0.4%.
References:
CN111170828,2020,A Location in patent:Paragraph 0022-0025
