2-TERT-BUTOXYCARBONYLAMINO-5-TRIFLUOROMETHOXY-BENZOIC ACID synthesis
- Product Name:2-TERT-BUTOXYCARBONYLAMINO-5-TRIFLUOROMETHOXY-BENZOIC ACID
- CAS Number:220107-35-7
- Molecular formula:C13H14F3NO5
- Molecular Weight:321.25
124-38-9
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Yield:220107-35-7 81%
Reaction Conditions:
Stage #1: tert-butyl N-(4-trifluoromethoxyphenyl)carbamatewith tert.-butyl lithium in tetrahydrofuran;pentane at -50; for 2 h;
Stage #2: carbon dioxide in tetrahydrofuran;pentane at 25;
References:
Leroux, Frederic;Castagnetti, Eva;Schlosser, Manfred [Journal of Organic Chemistry,2003,vol. 68,# 12,p. 4693 - 4699]
124-38-9
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$214.00/14L
220107-35-7
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$123.70/250mgs:
461-82-5
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$10.00/1g
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24424-99-5
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$13.50/25G
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34619-03-9
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220107-35-7
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