3,4-dihydroxy-5-iodobenzaldehyde synthesis
- Product Name:3,4-dihydroxy-5-iodobenzaldehyde
- CAS Number:54246-05-8
- Molecular formula:C7H5IO3
- Molecular Weight:264.02
5438-36-8
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Yield:54246-05-8 93%
Reaction Conditions:
Stage #1: 4-Hydroxy-3-iodo-5-methoxy-benzaldehydewith BBr3 in dichloromethane at 0 - 20; for 3 h;Inert atmosphere;
Stage #2: with methanol in dichloromethane at 0;
References:
Forli, Stefano;Holcomb, Matthew;Peters, David S.;Romesberg, Floyd E.;Santos-Martins, Diogo;Tan, Yun Xuan;Walsh, Shawn I. [Journal of Natural Products,2020,vol. 83,# 7,p. 2112 - 2121] Location in patent:supporting information