ChemicalBook CAS DataBase List 3,4-Dimethoxybenzyl alcohol

3,4-Dimethoxybenzyl alcohol synthesis

8synthesis methods

Product Name:3,4-Dimethoxybenzyl alcohol
CAS Number:93-03-8
Molecular formula:C9H12O3
Molecular Weight:168.19

Using 3,4-dimethoxybenzaldehyde as a raw material, reduction is carried out in methanol or other alcohol solvents by adding sodium borohydride (a mild reducing agent commonly used in industry), with the reaction stirred at room temperature to reflux temperature; or in the laboratory, lithium aluminum hydride (in anhydrous tetrahydrofuran or diethyl ether) can be used for reduction. After the reaction is completed, the product 3,4-dimethoxybenzyl alcohol is obtained by acidification, extraction, drying, distillation or recrystallization.

120-14-9 Synthesis

120-14-9
822 suppliers
$5.00/25g

93-03-8
416 suppliers
$5.00/1g

Yield:93-03-8 100%

Reaction Conditions:

with sodium tetrahydroborate in methanol at 20; for 1 h;

Steps:

Step-I (Preparation of benzyl alcohols)
General procedure: benzaldehyde derivatives (1 mmol) in methanol (15 mL), sodium borohydride (2 mmol) and stirred at room temperature for 1 h. Usual work-up, quantitative yield.

References:

Parihar, Swati;Kumar, Amit;Chaturvedi, Amit K.;Sachan, Naresh Kumar;Luqman, Suaib;Changkija, Bendangla;Manohar, Murli;Prakash, Om;Chanda;Khan, Feroz;Chanotiya;Shanker, Karuna;Dwivedi, Anila;Konwar, Rituraj;Negi, Arvind S. [Journal of Steroid Biochemistry and Molecular Biology,2013,vol. 137,p. 332 - 344]

FullText

1521-41-1
105 suppliers
$21.00/100mg

93-03-8
416 suppliers
$5.00/1g

References

2150-38-1
207 suppliers
$10.00/1g

93-03-8
416 suppliers
$5.00/1g

References

120-14-9 Synthesis

120-14-9
822 suppliers
$5.00/25g

23702-54-7
53 suppliers
$60.00/100mg

93-03-8
416 suppliers
$5.00/1g

References

93-07-2 Synthesis

93-07-2
561 suppliers
$5.00/5g

93-03-8
416 suppliers
$5.00/1g

References

3,4-Dimethoxybenzyl alcohol Related Search:

Veratraldehyde Benzyl alcohol 2,6-Dimethoxybenzaldehyde Veratric Acid 3-Phenoxybenzyl alcohol Diphenyldimethoxysilane Ethyl acetate 4,4'-DIMETHOXYBENZHYDROL Resveratrol m-Anisyl alcohol

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3,4-Dimethoxybenzyl alcohol synthesis

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