ChemicalBook CAS DataBase List 3,5-Dimethoxybenzylamine

3,5-Dimethoxybenzylamine synthesis

6synthesis methods

Product Name:3,5-Dimethoxybenzylamine
CAS Number:34967-24-3
Molecular formula:C9H13NO2
Molecular Weight:167.21

7 mmol of 3,5-dimethoxybenzaldehyde, 70 mL of methanol solution of ammonia at a concentration of 2 mol/L, and 140 mg of murrayne-encapsulated nickel-nickel oxide catalyst were mixed and added to an autoclave reactor, and then hydrogen was passed in, and t

7051-16-3 Synthesis

7051-16-3
208 suppliers
$10.00/1g

34967-24-3
167 suppliers
$13.00/1g

Yield:-

Steps:

Multi-step reaction with 2 steps
1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; sodium carbonate / 1,4-dioxane; water / 36 h / Reflux
2: ethylenediamine / 1,4-dioxane; propan-1-ol; water / 24 h / Reflux

References:

Murai, Norio;Miyano, Masayuki;Yonaga, Masahiro;Tanaka, Keigo [Organic Letters,2012,vol. 14,# 11,p. 2818 - 2821]

FullText

7311-34-4
335 suppliers
$10.00/1g

34967-24-3
167 suppliers
$13.00/1g

References

500-99-2
293 suppliers
$10.00/1g

34967-24-3
167 suppliers
$13.00/1g

References

17213-58-0
163 suppliers
$15.00/5g

34967-24-3
167 suppliers
$13.00/1g

References

34967-25-4
4 suppliers
inquiry

34967-24-3
167 suppliers
$13.00/1g

References

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3,5-Dimethoxybenzylamine synthesis

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