3-Chlorobenzoyl chloride synthesis
- Product Name:3-Chlorobenzoyl chloride
- CAS Number:618-46-2
- Molecular formula:C7H4Cl2O
- Molecular Weight:175.01
535-80-8
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$5.00/5g
618-46-2
358 suppliers
$9.00/25g
Yield:618-46-2 91%
Reaction Conditions:
with thionyl chloride for 2 h;Reflux;
Steps:
1.1 1) Preparation of Compound 1-1
3-chlorobenzoic acid (20 g, 128 mmol) was added to a solution ofAfter thionyl chloride (200 mL) was added, And the mixture was refluxed for 2 hours.After cooling to room temperature, distillation was performed, and the resulting solid was washed with diethylether and dried to obtain Compound 1-1. (20.3 g, 91% yield)
References:
LG Chem, Ltd.;Cho Seong-mi;Lee Jeong-ha;Lee Dong-hun;Park Tae-yun;Moon Jeong-uk;Jeong Min-u KR2018/55688, 2018, A Location in patent:Paragraph 0138; 0139; 0140; 0141
873-63-2
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618-46-2
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$9.00/25g
587-04-2
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618-46-2
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$9.00/25g
98-88-4
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618-46-2
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1128-76-3
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$8.00/1g
618-46-2
358 suppliers
$9.00/25g