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ChemicalBook CAS DataBase List 3-Dimethylaminoacrolein
927-63-9

3-Dimethylaminoacrolein synthesis

3synthesis methods
3-Dimethylaminoacrylaldehyde can be regarded as an amino-substituted unsaturated aldehyde compound, which can be prepared from N,N-dimethylformamide and ethyl alkenyl ether by condensation reaction.
-

Yield:75143-08-7 49%

Reaction Conditions:

with silica gel1,) 80 deg C to 90 deg C, 1.5 h, 2.) CHCl3, 1 h;

References:

Krasnaya, Zh. A.;Prokof'ev, E. P.;Kucherov, V. F. [Bulletin of the Academy of Sciences of the USSR Division of Chemical Science,1980,vol. 29,# 6,p. 987 - 990][Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya,1980,# 6,p. 1373 - 1376]

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