3-hydroxynaphthalene-2-carbaldehyde synthesis
- Product Name:3-hydroxynaphthalene-2-carbaldehyde
- CAS Number:581-71-5
- Molecular formula:C11H8O2
- Molecular Weight:172.18
56679-88-0
59 suppliers
$22.00/250mg
581-71-5
64 suppliers
$60.00/25mg
Yield: 99%
Reaction Conditions:
with aluminum (III) chloride in dichloromethane at 20; for 8 h;
Steps:
8
The compound was dissolved VII-1 (2mmol, 1equiv) 20mL of dichloromethane,An excess of AlCl3,In dry oxygen-free state holding 8h,The reaction was quenched with water and extracted with dichloromethane,After drying spin dry,A silica gel column (PE: EA = 8: 1),To give Compound VIII-1 (99%);
References:
East China University of Science and Technology;Wang, Limin;Wu, Xunshen;Yang, Yang;Wu, Shengying;Wang, Feng;Wang, Guifeng;Tian, He;Wang, Zhenyan;Chen, Lirong;Huang, Zhuo CN105601608, 2016, A Location in patent:Paragraph 0092; 0095
30159-70-7
38 suppliers
$45.00/50mg
581-71-5
64 suppliers
$60.00/25mg
92-70-6
444 suppliers
$10.00/10g
581-71-5
64 suppliers
$60.00/25mg
66-99-9
295 suppliers
$5.00/1g
581-71-5
64 suppliers
$60.00/25mg
39110-92-4
34 suppliers
$40.00/1g
581-71-5
64 suppliers
$60.00/25mg