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ChemicalBook CAS DataBase List 3-Methoxy-2-Nitro Benzonitrile
142596-50-7

3-Methoxy-2-Nitro Benzonitrile synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: SOCl2 / CH2Cl2 / 2 h / Heating
2: aq. NH3 / tetrahydrofuran / 0.5 h / Ambient temperature
3: 74.5 percent / SOCl2 / tetrahydrofuran / Ambient temperature

References:

Goto;Nakamura;Morioka;Kondo;Naito;Tsutsumi [Chemical and Pharmaceutical Bulletin,1996,vol. 44,# 3,p. 547 - 551]

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