Isovanillin synthesis
- Product Name:Isovanillin
- CAS Number:621-59-0
- Molecular formula:C8H8O3
- Molecular Weight:152.15
1131-52-8
281 suppliers
$6.00/5g
621-59-0
658 suppliers
$9.00/1g
Yield:621-59-0 97.2%
Reaction Conditions:
with water at 65; for 3 h;Large scale;Reagent/catalyst;Time;
Steps:
1.2; 2.2
(2) Add 728kg of intermediates, 150kg of SO42-/ZrO2-TiO2 catalyst, and 1500kg of water to the reactor, and react at 65°C for 3 hours to complete the reaction. Press filter the reaction solution, dissolve the filter cake with 2000kg ethanol, keep stirring at 60°C for 4h; press filter, transfer the filtrate to the crystallization kettle, lower the temperature to 0°C, keep stirring for 4h; Press filtration to obtain 631.23 kg of wet product, the filtrate is transferred to a rectification device, and the obtained solid is vacuum dried to a constant weight to obtain 593.21 kg of isovanillin.
References:
CN113185391,2021,A Location in patent:Paragraph 0019; 0031-0039; 0041-0051
4383-06-6
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$6.00/5g
621-59-0
658 suppliers
$9.00/1g
34841-06-0
249 suppliers
$8.00/5g
621-59-0
658 suppliers
$9.00/1g
123-11-5
902 suppliers
$10.00/10g
621-59-0
658 suppliers
$9.00/1g