5-Chloro-2-methyl-4-isothiazolin-3-one synthesis
- Product Name:5-Chloro-2-methyl-4-isothiazolin-3-one
- CAS Number:26172-55-4
- Molecular formula:C4H4ClNOS
- Molecular Weight:149.6
999-72-4
111 suppliers
$25.00/250mg
26172-55-4
413 suppliers
$15.00/1g
Yield:26172-55-4 95%
Reaction Conditions:
with chlorine;potassium iodide in ethyl acetate at 40 - 55; for 0.25 h;
Steps:
2 Example 2: Preparation of CMIT / MIT
N, N'-dimethyl-3,3'-dithiodipropionamide, ethyl acetate and potassium iodide were continuously fed into the preheating system at a ratio of 100: 500: 0.2,Preheat the mixture to 40 ~ 45 ° C.The solid-liquid mixture is uniformly mixed into a slurry through a static mixer, and then sent to a pipeline reactor for reaction. The pipeline reactor is fed with chlorine gas at multiple points and controlled by a temperature control system.The reaction temperature is 50 to 55 ° C, and the residence time is 15 minutes.After the reaction liquid from the pipeline reactor is separated by gas and liquid, it enters the post-processing system.After the post-treatment process, a 14% CMIT / MIT aqueous solution was obtained, the chlorine ratio was 3: 1, and the yield was 95%.During the process, all hydrogen chloride gas enters the hydrogen chloride absorption system to produce by-product hydrochloric acid.
References:
CN110483438,2019,A Location in patent:Paragraph 0018
999-72-4
111 suppliers
$25.00/250mg
26172-55-4
413 suppliers
$15.00/1g
2682-20-4
491 suppliers
$10.00/1g
52334-99-3
30 suppliers
inquiry
26172-55-4
413 suppliers
$15.00/1g
2682-20-4
491 suppliers
$10.00/1g
107-06-2
443 suppliers
$14.00/25g
26172-55-4
413 suppliers
$15.00/1g
1003-07-2
130 suppliers
$35.00/100mg
26172-55-4
413 suppliers
$15.00/1g