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ChemicalBook CAS DataBase List 4,4'-Cyclohexylidenebisphenol
843-55-0

4,4'-Cyclohexylidenebisphenol synthesis

9synthesis methods
In a 500 mL four-necked flask equipped with a PTFE stirrer, thermometer, reflux condenser and HCl gas introduction tube, 150.4 g (16 mol) of phenol, 39.2 g (0.4 mol) of cyclohexanone, 100 mL of toluene, and 624 g (008 mol) of 2-mercaptoethanol were added;
-

Yield:843-55-0 91%

Reaction Conditions:

with hydrogenchloride;cetyltrimethylammonium chloride;3-mercaptopropionic acid;sodium hydroxide in water for 4 h;

References:

Patil;Suryawanshi;Pawar;Shinde [E-Journal of Chemistry,2011,vol. 8,# 4,p. 2016 - 2019] Location in patent:experimental part

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