Phenol synthesis
- Product Name:Phenol
- CAS Number:108-95-2
- Molecular formula:C6H6O
- Molecular Weight:94.11
106-48-9
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108-95-2
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Yield:108-95-2 100%
Reaction Conditions:
with hydrogen;sodium hydroxide in lithium hydroxide monohydrate; under 760.051 Torr; for 0.833333 h;Kinetics;Green chemistry;Reagent/catalyst;Solvent;
Steps:
General procedures for the hydrodechlorination of CPs
General procedure: HDC experiments are performed in a three-necked jacketed glass reactor connected with hydrogen balloon by a three-wayvalve. Firstly, a certain quantity/amount of catalyst is placed into the mixed solution of 30 mL of solvent (H2O, ethyl acetate, ethylalcohol), 1 mmol of reactant and 1mmol base (Na2CO3, NaAc, triethyl amine, Na2OH). Secondly, use a circulating water vacuumpump to extract the air in the reactor for 5-10 s. Then open the three-way valve and make the hydrogen get into reactor. Repeating the gases replacement process three times and starting the clock. The reaction maintains for 2 h under vigorous stirring at room temperature. The results of the experiments are analysed by gas chromatograph-mass spectrometer (GC-MS).
References:
Liu, Yansheng;Qiao, Bo;Li, Xinlin;Le, Xuanduong;Zhang, Wei;Ma, Jiantai [Journal of Molecular Catalysis A: Chemical,2015,vol. 406,p. 65 - 71]
108-86-1
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108-95-2
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18052-27-2
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108-95-2
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120-80-9
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108-95-2
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4406-72-8
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108-95-2
779 suppliers
$14.00/25g