4-Acetylbenzonitrile synthesis
- Product Name:4-Acetylbenzonitrile
- CAS Number:1443-80-7
- Molecular formula:C9H7NO
- Molecular Weight:145.16
3032-92-6
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$28.00/1g
1443-80-7
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$6.00/1g
Yield:1443-80-7 92%
Reaction Conditions:
with chloro(1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene)gold(I);water in methanol at 110; for 6 h;
Steps:
15 Example 15 : 4-cyanoacetophenone
The catalyst [(IPr) AuCl] (6.2mg, 1mol%), 4- cyano-phenylacetylene (1mmol), in methanol (1ml) and water (0.5ml) was added successively 25ml reactor.After the reaction mixture was reacted for 6 hours at 110 , cooled to room temperature.Rotary evaporation to remove the solvent, then purified by column chromatography (eluent: petroleum ether / ethyl acetate) to give pure title compound, yield: 92%
References:
Nanjing University of Science and Technology;WANG, NANA;MA, JUAN;LI, FENG CN106032348, 2016, A Location in patent:Paragraph 0083-0086
3457-45-2
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$19.00/250mg
1443-80-7
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25309-65-3
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$12.00/1g
1443-80-7
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557-21-1
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$12.00/5g
109613-00-5
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$11.00/250mg
1443-80-7
357 suppliers
$6.00/1g